Service 02 · Deepest Specialisation · Every Thickener Chemistry

Grease Formulation
R&D — All Types

The most technically demanding area of lubricant chemistry — and our deepest specialisation since 2010. We formulate across every thickener system: soap-based (calcium, lithium, sodium, barium, aluminium), complex soaps (LiX, CaX, AlX, calcium sulfonate complex), non-soap (polyurea, bentone, silica, PTFE), and specialty types. Every formulation includes the complete manufacturing SOP — the process documentation is as critical as the formula itself.

15+
Thickener Chemistries
NLGI 000–6
All Consistency Grades
>260°C
Complex Soap Dropping Point
SOP Included
Every Formulation
NLGI Grade Reference

All Consistency Grades
We Formulate

ASTM D217 worked penetration (60 strokes) × 0.1mm

000
445–475
Semi-fluid
Enclosed gear cases, centralised lubrication systems
00
400–430
Semi-fluid
Enclosed gears, centralised systems, plain bearings
0
355–385
Very Soft
Centralised systems, gears, some bearings (low temperature)
1
310–340
Soft
Centralised lubrication, slow-speed bearings, steel mill
2
265–295
Standard
Most bearing applications — wheel bearings, electric motors, general industrial
3
220–250
Firm
Vertical or high-vibration applications, prevent slump
4
175–205
Very Firm
High vibration, hot applications where softer grease would leak
5–6
85–160
Block Grease
Open bearings, high-temp kiln, wire rope blocks, manual application
Complete Product Scope

Every Grease Type
We Formulate

Grease TypeThickener SystemDrop PointTemp RangeProperties, Applications & Notes
A · CALCIUM SOAP GREASES
Anhydrous Calcium GreaseCa-soap (12-HSA)~100°C–20°C to 80°CExcellent water resistance, smooth buttery texture, non-melt — stays in place near water. Low cost. Used in chassis lubrication, agricultural equipment, water-contact slow-speed bearings. Cannot be used above 80°C (drops at ~100°C).
Hydrated Calcium GreaseCa-soap (stearic)<80°C–10°C to 60°CContains ~1–3% water as structural stabiliser. Very soft, pumpable. Low-cost chassis, wheel bearings on slow vehicles. Being replaced by lithium grades in most applications but still widely used in India for very low-cost applications.
Calcium Cup GreaseCa-soap<80°C–10°C to 55°COld-style "cup grease" — used in agricultural and construction equipment cup bearings. Buttery, sticky. Designed for manual application via grease cups.
B · LITHIUM SOAP GREASES
Lithium Soap NLGI 1Li-12-HSA175–195°C–30°C to 130°CSoft multipurpose bearing grease. Used in centralised lubrication systems, low-temperature applications (cold stores, outdoor winter). Pumpable through lubrication lines.
Lithium Soap NLGI 2 — StandardLi-12-HSA175–200°C–25°C to 130°CThe world's most widely used grease. Multipurpose — automotive wheel bearings (front and rear), electric motor bearings, general-purpose industrial. Compatible with most seal types. Available in mineral, semi-synthetic, and full synthetic base.
Lithium Soap NLGI 2 — EP GradeLi-12-HSA + EP pkg185–205°C–25°C to 130°CEP additive added (sulfurized fat or MoS2). For loaded bearings, heavy industrial applications, mining. Four-ball EP weld point typically 200–250 kgf.
Lithium Soap NLGI 2 — Moly GradeLi-12-HSA + MoS₂185°C–25°C to 150°CMolybdenum disulfide (MoS2) added (2–10%). Platelet structure provides solid film lubrication under extreme load. Black colour. Used in slow-speed heavy-load applications, CV joints, splines, agricultural.
Lithium Soap NLGI 3Li-12-HSA185–200°C–20°C to 130°CFirmer consistency for high vibration or high-temperature applications where NLGI 2 would slump. Electric motor bearings in vertical orientation. High-speed spindle bearings.
C · LITHIUM COMPLEX GREASES
Lithium Complex NLGI 1/2/3 — MineralLi + azelaic/sebacic acid>260°C–30°C to 180°CDramatically higher drop point than lithium soap. Excellent EP capability, oxidation stability. BIS IS 7623 compliant. For steel mill roll neck bearings, heavy industrial gearbox output shaft bearings, hot-zone applications.
Lithium Complex — Semi-SyntheticLiX + Group III base>265°C–35°C to 190°CExtended high-temperature performance. Better oxidation stability than mineral LiX. For hot bearings in continuous operation (kiln drives, dryer bearings, baking oven conveyors at lower temperature).
Lithium Complex — Full Synthetic PAOLiX + PAO base>270°C–50°C to 200°CWidest temperature range. Excellent low-temperature pumpability (<–40°C). For cold-weather outdoor equipment, aerospace ground support, Arctic applications. Very long regreasing intervals.
Lithium Complex — Boric Acid TypeLi + boric acid>265°C–25°C to 180°CBoric acid as complexing agent instead of dibasic acid. Slightly different soap fibre structure — smoother texture. Good inherent EP and AW properties from borate.
D · CALCIUM COMPLEX GREASES
Calcium Complex NLGI 1/2/3Ca + acetic/boric acid>260°C–20°C to 180°COutstanding water washout resistance (better than LiX). High drop point. Excellent rust protection. Preferred for marine, mining, paper mills, offshore — anywhere with water ingress. D1264 water washout typically <5%.
Calcium Complex EP GradeCaX + EP pkg>260°C–20°C to 180°CHeavy EP package for mining shovels, steel plant roller bearings, continuous casting equipment. Water resistance makes it superior to LiX EP in wet environments.
E · CALCIUM SULFONATE COMPLEX GREASES
Calcium Sulfonate Complex NLGI 1/2Overbased Ca sulfonate>300°C (no drop)–20°C to 200°CNewest and most technologically advanced soap thickener. Inherent extreme pressure and rust protection from overbased calcium sulfonate structure — minimal additional additive required. Exceptional water washout (<1% D1264). True dropping point >300°C. For steel mills, paper mills, mining, marine — premium tier.
Calcium Sulfonate Complex — EP/AWCaSX + enhanced pkg>300°C–20°C to 200°CEnhanced EP additive package on top of inherent EP. For most severe heavy industrial applications. Four-ball weld point typically >400 kgf.
F · ALUMINIUM COMPLEX GREASES
Aluminium Complex NLGI 1/2Al soap + benzoic acid>240°C–25°C to 170°CHighly adhesive and tacky — unique property that prevents throw-off from high-speed or high-vibration applications. Excellent water resistance. Transparent to translucent appearance. Used for open gears, wire ropes, conveyor chains, slide ways.
Aluminium Complex — Wire Rope GreaseAlX + tackifier>240°C–20°C to 150°CEnhanced tackifier for maximum adhesion and penetration into wire rope core. Dark coloured (bitumen modified) or light variants. Mining headrope, crane wire, bridge cable applications.
G · SODIUM SOAP GREASES
Sodium Soap GreaseNa-stearate / Na-12-HSA140–165°C–10°C to 110°COlder thickener type — fibrous texture, not water-resistant. Limited to dry environments. Now largely replaced by lithium soap but still used in some industrial applications for its specific fibre structure properties. Emulsifies in water rather than resisting it.
H · POLYUREA GREASES
Diurea Grease NLGI 2Aliphatic diurea>250°C–30°C to 180°CHigh drop point, excellent oxidation stability (no soap = no metal salt catalysis). Not compatible with lithium or calcium soap greases. Long relubrication interval — used in electric motor sealed bearings (L10 life often 40,000+ hours). Very light colour, aesthetically clean.
Triurea Grease NLGI 2/3Aliphatic/aromatic triurea>260°C–25°C to 200°CHigher temperature capability than diurea. Aromatic triurea is used for high-temperature automotive wheel bearing applications (>160°C hub bearing temps). Requires specific synthesis conditions.
Polyurea — High-Speed Bearing GreaseDiurea + PAO/ester>250°C–40°C to 180°CLow-noise, precision bearing grease. Very low bleed (oil separation). For electric motors, textile spindle bearings, machine tool bearings at high speed. Excellent for sealed bearings (lifetime lubrication).
I · INORGANIC THICKENER GREASES
Bentone / Clay GreaseOrgano-clay (Hectorite)None (no drop)–30°C to 260°CTrue no-drop-point grease — does not melt at any temperature. Used for kiln bearings, oven chains, cement plant — applications above 200°C where soap greases fail. Requires solubiliser (propylene carbonate) for structure development. Very high initial cost but no alternative.
Silica Gel GreaseAmorphous silicaNone (no drop)–60°C to 280°CWidest temperature range of any thickener. Chemically inert — compatible with oxygen, strong oxidisers, reactive gases. For oxygen compressors, semiconductor, space applications. Used with PFPE base oil for ultimate performance. Very expensive specialty product.
PTFE Thickened GreasePTFE fibreNone (stable)–60°C to 250°CPTFE (Teflon) fibre suspension in PAO or silicone base. Very low friction coefficient, chemically inert, excellent for plastic and rubber contact applications. White grease for food machinery and pharmaceutical. Used in valve stems, threaded connections.
J · SPECIALTY & APPLICATION-SPECIFIC GREASES
Chassis Grease (Multi-Purpose)Li-soap or Ca-soap NLGI 2175–200°C–25°C to 130°CUniversal automotive chassis — king pins, tie rod ends, ball joints, U-joints. Water resistance, NLGI 2 for automatic grease gun. Low cost for high-volume automotive aftermarket.
Wheel Bearing GreaseLi or LiX NLGI 2/3185–260°C–30°C to 160°CHigh-speed wheel bearings — front and rear hub bearings. ASTM D1263 wheel bearing test leakage <20%. High drop point for drum brake heat. Corrosion protection for road splash. EP for loaded bearings.
Marine GreaseCaX or CaSX NLGI 1/2>260°C–20°C to 170°COutstanding water washout resistance — D1264 <3% at 79°C. Excellent salt spray corrosion resistance. For marine stern tubes, propeller shaft bearings, deck equipment, anchor windlasses, marine crane bearings.
Mining Grease — GeneralLiX or CaX NLGI 1/2>260°C–25°C to 180°CHigh EP (weld point >300 kgf), water resistance, vibration resistance. For conveyor systems, crushers, screens, draglines. Underground mining: additional fire resistance may be required (biodegradable ester base option).
Steel Mill GreaseLiX or CaSX NLGI 1/2>265°C–20°C to 190°CRoll neck bearings — extreme shock load, water quench, very high EP requirement. Four-ball weld >350 kgf. NLGI 1 for centralised lubrication system delivery. Water washout D1264 <5%.
Food Grade Grease NSF H1AlX or PTFE + white oil/PAO>235°C–30°C to 180°CAll ingredients on NSF approved substance list. White mineral oil or PAO base only. For food processing machinery bearings, conveyors, baking oven chains, packaging machinery. Non-toxic, odourless, tasteless.
Food Grade NSF H2LiX or standard thickener + white oil>240°C–25°C to 160°CFor food processing areas where there is no food contact risk. Registered NSF H2 — broader additive range allowed than H1. More economical than H1 for non-contact applications.
Food Grade NSF H3Edible oil baseN/A (soluble)Limited rangeSoluble/edible oils used to lubricate equipment where the lubricant is absorbed into food (e.g. baking pans). Not a conventional grease — separate formulation approach.
Open Gear GreaseBitumen + thickener NLGI 0/00N/A–10°C to 120°CVery high viscosity adhesive compound for large open gear drives — mining shovels, rotary kilns, cement mills, draglines. Bitumen/asphalt modified for adhesion. Spray application with diluent (solvent or hot applied). Gear rack pitch lubrication.
Extreme Temperature Grease (>200°C)Bentone + PAO/PFPE or CaSXNo dropup to 280°C continuousApplications above 200°C continuous — kiln trunnion bearings (cement, lime), glass furnace annealing lehr, tunnel oven chain bearings. Bentone or CaSX thickener in synthetic base. Very long relubrication intervals justified by access difficulty.
Low Temperature Grease (<–40°C)LiX or diurea + PAO>250°C–60°C to 150°CArctic and cold store applications. PAO base for pour point <–50°C. Low viscosity base oil (PAO 4cSt at 40°C) for pumpability at low temperature. Used in outdoor bearings (antenna drives, gate valves), cold stores, refrigeration.
Electric Motor GreasePolyurea NLGI 2/3>250°C–30°C to 180°CLow noise (acoustic grease). Excellent oxidation stability for long service life in sealed bearings. Rust inhibition for moisture from condensation cycling. Polyurea preferred — no soap metal ions that can corrode winding insulation.
CV Joint / Drive Shaft GreaseLi or LiX NLGI 1/2 + MoS₂/EP>185°C–40°C to 150°CConstant velocity joints — plunge and fixed types. Very high EP and AW at slow-speed articulation angles. MoS2 or organic sulfur EP for boundary lubrication. Must not crack or harden at low temperature. Compatible with rubber boots.
Railway Bearing GreaseLiX or polyurea NLGI 2/3>260°C–40°C to 180°CRailway axle box bearings — Indian Railways RDSO specification. Extreme shock load resistance. Water washout critical (rain and track washing). AAR M-942 (freight), ABMA high-speed passenger. Long service intervals (150,000–300,000 km).
Flange / Curve GreaseBitumen or CaSX basedN/A (adhesive)Rail track useApplied to rail flange or wheel flange to reduce wear on curves. Very adhesive, high film strength. Controlled friction coefficient for traction maintenance. Applied by wayside applicators or onboard systems.
Aviation GreasePolyurea or LiX + PAO/ester>250°C–65°C to 200°CAerospace and defence aircraft applications. MIL-PRF-23827 (general purpose), MIL-PRF-81322 (wide temperature, wheel bearings), MIL-PRF-32014 (extreme pressure). PAO/ester base for low-temperature and oxidation performance. Very stringent qualification testing.
Anti-Corrosion GreaseLi or Ca soap + heavy rust pkg>175°CBroad rangeLong-term corrosion protection for stored parts, threaded fasteners, pipe connections, flanges. High petroleum sulfonate and wax content. Salt spray resistance (ASTM B117) >500 hours. Slow-moving or stationary applications.
Dielectric Grease (Connector Grease)Silicone or PTFEStable to 260°C–60°C to 260°CNon-conductive grease for electrical connectors, spark plug boots, battery terminals. Prevents oxidation and moisture ingress. Silicone base for highest temperature range. Compatible with rubber and plastic connector housings.
Thread Compound (Anti-Seize)Li soap + metallic flakes>180°C–30°C to 1200°CCopper, nickel, or zinc flake filled compounds for high-temperature threaded connections — flanges, exhaust systems, boiler fittings, oil well casing. Prevents galling and seizing. Nickel-based for highest temp (1200°C continuous).
Penetrating GreaseLi soap NLGI 00/0 + penetrant>175°C–20°C to 110°CVery soft consistency for penetration into corroded and seized bearings, chains, slide mechanisms. Capillary-active additive for penetration. Rust converter chemistry. Primarily for maintenance use.
What We Deliver

Formula + SOP + Testing:
The Complete Package

Formulation Document
  • Base oil: group, grade, viscosity, and blend ratio by weight %
  • Fatty acid type (12-HSA, stearic, oleic), purity, source specification
  • Alkali: type (LiOH·H2O, Ca(OH)2), stoichiometric ratio to fatty acid
  • Complexing acid: type, purity, ratio to soap (for complex greases)
  • All additives: EP, AW, antioxidant, rust inhibitor — type and wt%
  • Final formula balanced to target NLGI penetration range
Manufacturing SOP
  • Step-by-step saponification — exact addition sequence and conditions
  • Temperature profile: ramp rates, hold temperatures, hold durations
  • Quench and cooling procedure with temperature checkpoints
  • Additive addition sequence, temperatures, and mixing times
  • Milling: pass count, pressure settings, expected viscosity change
  • Penetration control: how to adjust consistency during production
ASTM Testing
  • ASTM D217 — penetration worked/unworked, 60 strokes and 10,000 strokes
  • ASTM D566/D2265 — dropping point (low and high temperature)
  • ASTM D1264 — water washout at 38°C and 79°C
  • ASTM D4172 — four-ball wear scar diameter
  • ASTM D2783 — four-ball EP weld point and Load Wear Index
  • ASTM D942 — oxidation stability (oxygen bomb)
  • ASTM D1743 — corrosion in bearings
Documentation
  • Technical Data Sheet with all ASTM typical values
  • Safety Data Sheet (SDS/MSDS) — GHS 16-section format
  • BIS IS 7623 test data package (if required)
  • NSF H1 ingredient compliance check (if food grade)
  • Production batch QC acceptance protocol
  • Shelf life guidance and storage recommendations
Case Study

LiX NLGI 1/2/3 — Steel Mill
Drop Point >268°C, Certified

Completed Project · Lithium Complex Grease
NLGI 1, 2 & 3 Lithium Complex — EP Grade, Steel Mill Application, BIS IS 7623
A Gujarat grease manufacturer needed three NLGI grades (1, 2, 3) of lithium complex grease for a steel mill customer requiring drop point >260°C, four-ball EP weld point >250 kgf, and water washout <15% at 79°C. We designed a unified LiX base using azelaic acid as complexing agent with Indian-sourced 12-hydroxystearic acid, Group II base oil, and a combined sulfurised fat / antioxidant / rust inhibitor additive package — allowing all three grades to share the same soap concentrate, with milling used to achieve the target NLGI grade.
Dropping Point
>268°C — exceeds spec
Four-Ball EP Weld
315 kgf — far exceeds limit
Water Washout @ 79°C
9.8% — well within 15% limit
BIS IS 7623
All 3 grades certified
Common Questions

Frequently Asked
About Grease Formulation

Is the SOP specific to my reactor or generic?

Specific to your reactor. We ask about volume, jacket type (steam, thermal oil, electric), stirrer speed, chilling capability, and material (stainless vs mild steel). Temperature hold times and heating rates are particularly equipment-dependent. A 200 kg electric-heated reactor behaves very differently from a 400 kg steam-jacketed reactor at the same saponification stage.

What is the difference between calcium sulfonate complex and lithium complex, and when do I choose one over the other?

Calcium sulfonate complex (CaSX) has several inherent advantages over lithium complex (LiX): it provides EP and rust protection without additives (from the overbased sulfonate structure), has no true drop point (>300°C), and has outstanding water washout resistance (<1% D1264). However, it is more difficult and expensive to manufacture — requires high-quality overbased calcium sulfonate raw material and a specific conversion process to achieve gel structure.

Choose LiX when: cost is the primary driver, standard EP performance is sufficient, and your operators are already experienced with saponification. Choose CaSX when: the application has severe water exposure (marine, paper mill, mining), when maximum EP performance with minimum additive treat rate is required, or when the specification demands drop point >300°C. We can formulate both and advise on the economically optimal choice for your specific application and market.

Can you formulate polyurea grease and what manufacturing equipment does it require?

Yes. Polyurea grease synthesis differs fundamentally from soap grease — it is produced by reacting isocyanate (MDI or TDI) with an amine (aliphatic or aromatic) in base oil. No saponification reactor is required in the traditional sense — but the reaction is exothermic and requires careful temperature control to prevent runaway.

Equipment: a jacketed reactor with temperature control and good agitation, plus a milling step. The process is shorter than soap saponification but the raw materials (isocyanate) require proper safety handling (moisture exclusion, PPE, ventilation). We provide complete synthesis SOP and safety protocol.

We are experiencing oil separation (bleeding) in our grease. Can you help diagnose and fix it?

Yes — oil bleeding (oil separation) is a very common problem. Root causes: (1) base oil viscosity too low for the soap content — the oil is not adequately retained in the soap matrix; (2) soap content too low — insufficient thickener for the base oil viscosity; (3) insufficient milling — soap fibres not adequately dispersed; (4) base oil polarity mismatch with soap thickener type.

Share your formula, base oil specs, and ASTM D1742 (or D6184) oil separation test results. We diagnose the root cause and provide specific corrective actions — usually resolvable with formulation adjustment rather than a complete redesign.

Can grease of different thickener types be mixed (compatibility)?

Grease compatibility is a critical issue when switching products in a lubrication system. Some combinations are compatible, some incompatible, and some are unpredictable. Incompatible greases, when mixed, can produce a softer mixture that leaks out of bearings — causing premature failure.

As a guide: Lithium + Lithium Complex = generally compatible. Lithium + Polyurea = incompatible (softens dramatically). Calcium soap + Lithium = conditionally compatible. Calcium Sulfonate Complex + most types = generally compatible. Bentone + most types = test required. We provide specific compatibility guidance for any combination you are evaluating and can conduct ASTM D6185 compatibility testing.

What is the minimum plant investment needed to produce lithium grease?
A minimum viable 200 kg batch lithium soap grease plant — jacketed electric-heated reactor, drum filter, hand-filling station, penetrometer — can be set up for ₹35–50 lakh from Indian fabricators. We advise on reactor specification, equipment sourcing, and complete plant design as part of our Plant Setup service. Calcium grease requires less stringent temperature control than lithium and is even simpler to start with.
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